Modular In Situ Electrochemical Cell, Model: EC-MOD

Description

Product Description

The EC-MOD is a modular flow-through electrochemical cell designed to couple three-electrode control with in situ spectroscopy and diffraction. Interchangeable optical and X-ray window assemblies configure the same base cell for Raman, FTIR, UV–Vis, XRD, or XAS measurements. Standard plate-electrode and gas-diffusion configurations support liquid-phase interfacial studies, spectroelectrochemical analysis, and gas-fed electrocatalytic reactions.

Key Features

  • Multi-technique Window Platform: Interchangeable quartz, sapphire, CaF₂, Kapton film and beryllium windows configure the cell for different in situ analytical methods.
  • Dual Working Electrode Configurations: Standard plate-electrode and gas-diffusion assemblies support conventional liquid-phase studies and gas-fed electrocatalysis.
  • Flow-Through Electrolyte Circulation: Dedicated inlet and outlet ports support external electrolyte circulation and controlled flow during electrochemical measurements.

Technical Specifications

Cell configuration < 1.5 mm
Optical window size 15 × 15 mm
Chamber structure Single-chamber (standard configuration); Two-chamber (gas-diffusion configuration)
Working electrode Sheet-type electrode
Reference electrode Ag/AgCl electrode (standard)
Counter electrode Platinum wire electrode
Cell body material PEEK + Ti
Raman/UV-Vis windows Sapphire (standard) or quartz (optional)
XAFS window Kapton film (optional)
XRD window Beryllium (optional)
IR window CaF₂ (ZnSe optional)

Instrument Compatibility

  • Spectroscopy and X-ray Compatibility: Configurable for Raman, UV–Vis, and IR optical systems, synchrotron XAFS beamlines, and laboratory or synchrotron XRD instruments, subject to instrument geometry, beam size, incidence angle, optical access, and working-distance requirements.
  • Electrochemical and Flow System Compatibility: Compatible with standard three-electrode potentiostats, external electrolyte pumps, PTFE tubing, gas-supply systems and downstream product-collection equipment.

Standard and Gas-Diffusion Configurations

 

  • Standard Configuration (single-chamber)

 

General Test Configuration

IR Test Configuration

  • Gas-diffusion Configuration (two-chamber)

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