In Situ XRD Electrochemical Cell, Model: EC-XRD1

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Description

Product Description

The EC-XRD1 provides direct X-ray access to an interchangeable disk working electrode through an X-ray-transparent beryllium (Be) window while maintaining three- electrode electrochemical control. Its compact flow-compatible design supports both syringe filling and external electrolyte circulation, making it suitable for tracking phase transformations and structural evolution of electrode materials under applied electrochemical conditions.

Product Features

  • Direct Structural Observation: Be-window access and a short X-ray path enable direct probing of the working-electrode surface.
  • Flexible Disk-Electrode Selection: Uses a standard Ø5 mm glassy carbon disk and supports interchangeable Au, Pt, Ag, graphite, and pyrolytic graphite disks.
  • Operando Phase-Evolution Analysis: Enables potential- and time-dependent monitoring of crystalline phase transformations and structural evolution of electrode materials.

Technical Specifications

WE-optical window distance < 3 mm
Optical window diameter Ø25 mm (effective diameter Ø20 mm)
Chamber structure Single-chamber
Electrode system Three-electrode
Working electrode Ø5 mm glassy carbon disk electrode (standard); Au, Pt, Ag, graphite, or pyrolytic graphite disk electrodes (optional)
Reference electrode Ag/AgCl or Ag/Ag⁺ electrode
Counter electrode Ø1 mm Platinum wire electrode
Cell body material PEEK + Ti
Optical window material Beryllium (Be)
Cell body dimensions L65 × W65 × H19 mm

Note: Solid beryllium is relatively stable and poses low skin-contact risk; avoid inhaling dust or aerosols and wash hands after handling.

Instrument Compatibility

  • XRD System Compatibility: Compatible with laboratory X-ray diffractometers that accommodate external electrochemical cells. Measurement geometry, sample-stage clearance, and mounting should be confirmed before use.
  • Potentiostat Compatibility: Compatible with commercial three-electrode potentiostats for electrochemical control during operando XRD measurements.

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